(2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Base Information

Chemical Name:(2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester
CAS No.:201798-53-0
Molecular Formula:C₁₅H₂₃NO₅S
Molecular Weight:329.417
Hs Code.:

Synonyms:(2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

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Chemical Property of (2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

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Technology Process of (2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

There total 2 articles about (2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 185015-76-3
(4S,5R)-4-Isobutyl-2-oxo-3-(toluene-4-sulfonyl)-oxazolidine-5-carboxylic acid (1R,2S)-2-phenyl-cyclohexyl ester

: 201798-53-0
(2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Guidance literature:: With methanol; potassium carbonate; for 6h; Ambient temperature;
DOI:10.1016/S0957-4166(97)00595-8

Reference yield:

: (R)-4-(1-Iodo-2-methyl-propyl)-2-oxo-3-(toluene-4-sulfonyl)-oxazolidine-5-carboxylic acid (1R,2S)-2-phenyl-cyclohexyl ester

: 201798-53-0
(2R,3S)-2-Hydroxy-5-methyl-3-(toluene-4-sulfonylamino)-hexanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / AIBN, Bu₃SnH / benzene / 1 h / Heating

2: 96 percent / K₂CO₃, methanol / 6 h / Ambient temperature

With methanol; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; In benzene;
DOI:10.1016/S0957-4166(97)00595-8