2-azatricyclo[3.3.1.13,7 ]decane

Base Information

• Chemical Name: 2-azatricyclo[3.3.1.13,7 ]decane
• CAS No.: 768-41-2
• Molecular Formula: C₉H₁₅N
• Molecular Weight: 137.225

Synonyms:2-azatricyclo[3.3.1.13,7 ]decane

Chemical Property of 2-azatricyclo[3.3.1.13,7 ]decane

Chemical Property:

• Melting Point: 224-227 °C(bomb tube)
• Boiling Point: 214.5±8.0 °C(Predicted)
• Density: 1.012±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

2-Azaadamantane 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-azatricyclo[3.3.1.13,7 ]decane

There total 45 articles about 2-azatricyclo[3.3.1.13,7 ]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-aza-tricyclo[3.3.1.1.3.7]decane-2-carboxylic acid methyl ester → 2-azatricyclo[3.3.1.13,7 ]decane (768-41-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 90 ℃; for 8h; Sealed tube;

Reference yield: 92.0%

2-azatricyclo[3.3.1.13,7]decan-2-ol (1155843-79-0) → 2-azatricyclo[3.3.1.13,7 ]decane (768-41-2)

Guidance literature:

With hydrogen; In ethanol; water; at 25 ℃; for 4h; under 760.051 Torr;

DOI:10.1002/anie.201706594

Reference yield: 88.0%

N-(2-nitrophenylsulfonyl)-2-azaadamantane (1155843-83-6) → 2-azatricyclo[3.3.1.13,7 ]decane (768-41-2)

Guidance literature:

With potassium carbonate; thiophenol; In toluene; at 50 ℃;

upstream raw materials:

(1s,3s,5R,7S)-1-chloro-2-azaadamantane

7,7-ethylenedioxybicyclo[3.3.1]nonan-3-one oxime

N-benzyloxycarbonyl-2-azaadamantane-1-ol

1-Hydroxy-2-aza-adamantan

Downstream raw materials:

2-azatricyclo[3.3.1.1^3,7]dec-2-yloxidanyl

2-azaadamantane-N-oxyl

N-benzyl-2-azatricyclo[3.3.1.13,7]decane

C₁₇H₁₈F₃NO

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