Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI)

Base Information

Chemical Name:Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI)
CAS No.:196699-09-9
Molecular Formula:C₉H₁₉NO
Molecular Weight:157.256
Hs Code.:
Mol file:196699-09-9.mol

Synonyms:Cyclohexanamine,2-methoxy-N,N-dimethyl-, trans-; trans-1-(Dimethylamino)-2-methoxycyclohexane

Suppliers and Price of Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI)

Chemical Property:

PSA：12.47000
LogP:1.50560

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI)

There total 5 articles about Cyclohexanamine, 2-methoxy-N,N-dimethyl-, (1R,2R)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Trimethyl-(2c-hydroxy-cyclohexyl-(1r))-ammonium-hydroxyd

: 196699-09-9
2c-Dimethylamino-1r-methoxy-cyclohexan

Guidance literature:: at 150 - 155 ℃;
DOI:10.1021/ja00872a025

Reference yield:

: tert-butyl (1S,2S)-2-methoxycyclohexyl(methyl)carbamate

: 196699-09-9
(1S,2S)-2-methoxy-N,N-dimethylcyclohexanamine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; Reflux;
DOI:10.1021/acs.joc.0c00832

Reference yield:

: 21651-84-3
trans-2-(methylamino)cyclohexanol

: 196699-09-9
(1S,2S)-2-methoxy-N,N-dimethylcyclohexanamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 30 °C

2: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C

3: lithium aluminium tetrahydride / diethyl ether / 0 °C / Reflux

With lithium aluminium tetrahydride; sodium hydride; sodium hydroxide; In tetrahydrofuran; diethyl ether; water; mineral oil;
DOI:10.1021/acs.joc.0c00832