1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

Base Information

Chemical Name:1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin
CAS No.:129957-68-2
Molecular Formula:C₁₉H₂₁NO₅
Molecular Weight:343.379
Hs Code.:

Synonyms:1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

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Chemical Property of 1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

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Technology Process of 1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

There total 2 articles about 1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 129957-60-4
1-Ethoxycarbonyl-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

: 129957-68-2
1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; at 60 ℃; for 4h;
DOI:10.1002/ardp.19903230610

Reference yield:

: 2739-98-2
ethyl 2-(pyridinyl-2)acetate

: 129957-68-2
1-Ethoxycarbonyl-6,7,8,9-tetrahydro-2-hydroxy-3-(4-methoxyphenyl)-4-oxo-4H-chinolizin

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / various solvent(s) / 0.25 h / Heating

2: 85 percent / H₂ / 5percent Pd/C / acetic acid / 4 h / 60 °C

With hydrogen; palladium on activated charcoal; In acetic acid;
DOI:10.1002/ardp.19903230610