Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-acetyl-, [1R-(endo,endo)]- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-acetyl-, [1R-(endo,endo)]- (9CI)
• CAS No.: 196618-85-6
• Molecular Formula: C₁₀H₁₂O₂
• Molecular Weight: 164.204
• Mol file: 196618-85-6.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde,3-acetyl-, [1R-(endo,endo)]- (9CI)

Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-acetyl-, [1R-(endo,endo)]- (9CI)

Chemical Property:

• PSA: 34.14000
• LogP: 1.21260

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-acetyl-, [1R-(endo,endo)]- (9CI)

There total 2 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 3-acetyl-, [1R-(endo,endo)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,2R,3R,4S,5S,6R)-3-Methyl-tricyclo[4.2.1.02,5]non-7-ene-3,4-diol (196607-63-3) → (1R,2S,3R,4S)-3-Acetyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde (196618-85-6,220191-57-1,220191-58-2,587875-56-7)

Guidance literature:

With sodium periodate; In dichloromethane;

DOI:10.1039/a702910a

Reference yield:

(1S,2R,3R,4S,5S,6R)-3-Methyl-tricyclo[4.2.1.02,5]non-7-ene-3,4-diol (196607-63-3) → (1R,2S,3R,4S)-3-Acetyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde (196618-85-6,220191-57-1,220191-58-2,587875-56-7) + (1S,2R,3S,4R)-3-Acetyl-bicyclo[2.2.1]hept-5-ene-2-carbaldehyde (220191-57-1,220191-58-2,587875-56-7)

Guidance literature:

With sodium periodate; Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(97)01488-3

upstream raw materials:

(1S,2R,3R,4S,5S,6R)-3-Methyl-tricyclo[4.2.1.0^2,5]non-7-ene-3,4-diol

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