5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

Base Information

Chemical Name:5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine
CAS No.:752232-91-0
Molecular Formula:C₄₈H₄₆N₂O₁₀Si
Molecular Weight:838.986
Hs Code.:

Synonyms:5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

Chemical Property:

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Technology Process of 5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

There total 2 articles about 5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 752232-87-4
5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-uracil

: 752232-91-0
5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

Guidance literature:: With chloro-trimethyl-silane; tin(IV) chloride; 1,1,1,3,3,3-hexamethyl-disilazane; In acetonitrile;
DOI:10.1039/b404150j

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 752232-91-0
5-[2-(tert-butyldiphenylsilanyloxy)ethyl]-2',3',5'-tri-O-benzoyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazole / dimethylformamide / 17.5 h / 20 °C

2: 60 percent / hexamethyldisilazane; Me₃SiCl; SnCl₄ / acetonitrile

With 1H-imidazole; chloro-trimethyl-silane; tin(IV) chloride; 1,1,1,3,3,3-hexamethyl-disilazane; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b404150j