methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

Base Information

• Chemical Name: methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate
• CAS No.: 944164-50-5
• Molecular Formula: C₁₂H₁₂N₄O₄
• Molecular Weight: 276.252
• Mol file: 944164-50-5.mol

Synonyms:methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

Chemical Property of methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

Chemical Property:

Purity/Quality:

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Technology Process of methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

There total 1 articles about methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

3-methyl-5-aminopyrazole (31230-17-8) + 4-fluoro-3-nitro-benzoic acid methyl ester (329-59-9) → methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate (944164-50-5)

Guidance literature:

In dimethyl sulfoxide; at 24.85 ℃; for 2h;

DOI:10.1107/S0108270106044611

Reference yield: 92.0%

methyl 3-nitro-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate (944164-50-5) → methyl 3-amino-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate (944164-52-7)

Guidance literature:

With hydrazine hydrate; nickel; In methanol; for 0.25h; Heating;

DOI:10.1107/S0108270106044611

upstream raw materials:

3-methyl-5-aminopyrazole

4-fluoro-3-nitro-benzoic acid methyl ester

Downstream raw materials:

methyl 3-amino-4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate