Technology Process of C25H19N(18)O
There total 6 articles about C25H19N(18)O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,10-Phenanthroline; water; copper diacetate; oxygen-18;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 5h;
under 760.051 Torr;
DOI:10.1021/ol301583y
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diethyl ether / 2 h / 80 °C / Cooling with ice
1.2: 0 °C
2.1: 1,10-Phenanthroline; water; copper diacetate; oxygen-18 / N,N-dimethyl-formamide / 5 h / 20 °C / 760.05 Torr
With
1,10-Phenanthroline; water; copper diacetate; oxygen-18;
In
diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ol301583y
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydroxylamine hydrochloride / dimethyl sulfoxide / 3 h / 100 °C
2.1: diethyl ether / 2 h / 80 °C / Cooling with ice
2.2: 0 °C
3.1: 1,10-Phenanthroline; water; copper diacetate; oxygen-18 / N,N-dimethyl-formamide / 5 h / 20 °C / 760.05 Torr
With
1,10-Phenanthroline; hydroxylamine hydrochloride; water; copper diacetate; oxygen-18;
In
diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol301583y