methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

Base Information

Chemical Name:methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate
CAS No.:150461-15-7
Molecular Formula:C₃₆H₃₅ClN₂O₂S₂
Molecular Weight:627.271
Hs Code.:

Synonyms:methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

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Chemical Property of methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

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Technology Process of methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

There total 14 articles about methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3256-88-0
5-phenyl-2-picoline

: 150461-15-7
methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / N-chlorosuccinimide, benzoyl peroxide / CCl₄ / 5 h / Heating; Irradiation

2: 69 percent / Et₃N / tetrahydrofuran / Ambient temperature

3: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 0 deg C, 75 min

With N-chloro-succinimide; Perbenzoic acid; sodium hydride; triethylamine; In tetrahydrofuran; tetrachloromethane;
DOI:10.1021/jm00071a008

Reference yield:

: 146775-28-2
2-chloromethyl-5-phenylpyridine

: 150461-15-7
methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / Et₃N / tetrahydrofuran / Ambient temperature

2: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 0 deg C, 75 min

With sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00071a008

Reference yield:

: 147936-58-1
5-phenyl-2-picoline N-oxide

: 150461-15-7
methyl 3-<1-(4-chlorobenzyl)-4-methyl-6-<<(5-phenylpyridin-2-yl)methyl>thio>-4,5-dihydro-1H-thiopyrano<2,3,4-c,d>indol-2-yl>-2,2-dimethylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / phosphoryl chloride, Et₃N / CH₂Cl₂

2: 69 percent / Et₃N / tetrahydrofuran / Ambient temperature

3: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 0 deg C, 75 min

With sodium hydride; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00071a008