2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Base Information

Chemical Name:2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon
CAS No.:103669-94-9
Molecular Formula:C₂₈H₃₂ClNO₁₂
Molecular Weight:610.015
Hs Code.:

Synonyms:2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

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Chemical Property of 2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Chemical Property:

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Technology Process of 2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

There total 4 articles about 2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

: 103669-74-5
N-(2,3,4,5,6-Penta-O-acetyl-D-gluconoyl)-DL-2-phenylglycin-3-chlor-2-butenylester

: 103669-94-9
2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

: 103670-08-2
Acetic acid (1R,2S,3R,4R)-2,3,4,5-tetraacetoxy-1-[4-(1-chloro-1-methyl-allyl)-5-oxo-4-phenyl-4,5-dihydro-oxazol-2-yl]-pentyl ester

Guidance literature:: With hexachloroethane; triethylamine; triphenylphosphine; In acetonitrile; at 95 - 100 ℃; for 1h;

Reference yield:

: 53555-69-4
2,3,4,5,6-penta-O-acetyl-D-gluconoyl chloride

: 103669-94-9
2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / CH₂Cl₂ / 2 h / 25 °C

2: 92.5 percent / dicyclohexylamine / tetrahydrofuran / 15 h / Heating

3: triphenylphosphane, triethylamine, C₂Cl₆ / acetonitrile / 1 h / 95 - 100 °C

With hexachloroethane; triethylamine; N-cyclohexyl-cyclohexanamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 75247-41-5
N-Trimethylsilyl-DL-2-phenylglycin-trimethylsilylester

: 103669-94-9
2-(3-Chlor-2-butenyl)-2-(1,2,3,4,5-pentaacetoxy-D-gluco-pentyl)-4-phenyl-5(2H)-oxazolon

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / CH₂Cl₂ / 2 h / 25 °C

2: 92.5 percent / dicyclohexylamine / tetrahydrofuran / 15 h / Heating

3: triphenylphosphane, triethylamine, C₂Cl₆ / acetonitrile / 1 h / 95 - 100 °C

With hexachloroethane; triethylamine; N-cyclohexyl-cyclohexanamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile;