Benzyl-PEG7-amino

Base Information

• Chemical Name: Benzyl-PEG7-amino
• CAS No.: 868594-43-8
• Molecular Formula: C₂₁H₃₇NO₇
• Molecular Weight: 415.527
• Mol file: 868594-43-8.mol

Synonyms:20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosylamine

Chemical Property of Benzyl-PEG7-amino

Chemical Property:

Purity/Quality:

99%+, ^*data from raw suppliers

BnO-PEG6-CH2CH2NH2 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-PEG7-amino

There total 1 articles about Benzyl-PEG7-amino which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-azido-20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosane (868594-42-7) → 20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosylamine (868594-43-8)

Guidance literature:

1-azido-20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosane; With triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 3h;

With water; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1002/ejoc.200701188

Reference yield:

20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosylamine (868594-43-8) → 2-[2-[2-[2-[2-[2-(2-aminoethoxy)ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethanol

Guidance literature:

With ammonia; sodium; In diethyl ether; at -78 - -30 ℃; Inert atmosphere;

DOI:10.1002/ejoc.200701188

upstream raw materials:

1-azido-20-(phenylmethyloxy)-3,6,9,12,15,18-hexaoxaeicosane

Refernces