tert-butyl phenethyl(piperidin-4-yl)carbamate

Base Information

Chemical Name:tert-butyl phenethyl(piperidin-4-yl)carbamate
CAS No.:934695-79-1
Molecular Formula:C₁₈H₂₈N₂O₂
Molecular Weight:304.433
Hs Code.:

Synonyms:tert-butyl phenethyl(piperidin-4-yl)carbamate

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Chemical Property of tert-butyl phenethyl(piperidin-4-yl)carbamate

Chemical Property:

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Technology Process of tert-butyl phenethyl(piperidin-4-yl)carbamate

There total 8 articles about tert-butyl phenethyl(piperidin-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.5%

: tert-butyl (1-benzylpiperidin-4-yl)(phenethyl)carbamate

: 934695-79-1
tert-butyl phenethyl(piperidin-4-yl)carbamate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 40 ℃;

Reference yield:

: 64-04-0
phenethylamine

: 934695-79-1
tert-butyl phenethyl(piperidin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium cyanoborohydride; acetic acid / methanol / 3 h / Cooling with ice

2: sodium hydrogencarbonate / tert-butyl alcohol; water / Cooling with ice

3: palladium 10% on activated carbon; hydrogen / methanol / 50 °C / 15001.5 Torr

With palladium 10% on activated carbon; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; In methanol; water; tert-butyl alcohol; 1: |Borch Reduction;
DOI:10.1016/j.ejmech.2018.05.027

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 934695-79-1
tert-butyl phenethyl(piperidin-4-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium cyanoborohydride; acetic acid / methanol / 3 h / Cooling with ice

2: sodium hydrogencarbonate / tert-butyl alcohol; water / Cooling with ice

3: palladium 10% on activated carbon; hydrogen / methanol / 50 °C / 15001.5 Torr

With palladium 10% on activated carbon; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate; acetic acid; In methanol; water; tert-butyl alcohol; 1: |Borch Reduction;
DOI:10.1016/j.ejmech.2018.05.027