2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Base Information

Chemical Name:2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide
CAS No.:89882-58-6
Molecular Formula:C₂₅H₂₇NOS
Molecular Weight:389.561
Hs Code.:

Synonyms:2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Suppliers and Price of 2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Chemical Property:

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Technology Process of 2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

There total 5 articles about 2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 591-51-5
phenyllithium

: 79250-30-9
4,4-diphenyl-2-t-butylisothiazolidin-3-one

: 89882-58-6
2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Guidance literature:: In diethyl ether; for 0.5h; from -78 deg C to room temp.;

Reference yield:

: 53216-38-9
2,2 diphenyl-3-mercapto-propionic acid

: 89882-58-6
2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / iodine, sodium hydroxide, potasium iodide, sodium sulphide / methanol

2: triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

3: 70 percent / pyridine, bromine / CH₂Cl₂ / from -78 deg C to room temp.

4: 82 percent / diethyl ether / 0.5 h / from -78 deg C to room temp.

With pyridine; sodium sulfide; sodium hydroxide; bromine; iodine; triethylamine; potassium iodide; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 97759-71-2
2,2-diphenyl-3-phenylsulfanyl-propionic acid

: 89882-58-6
2,2-diphenyl-3-phenylthio-N-t-buthylpropionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / thionyl chloride

2: 82 percent / diethyl ether / 0.5 h / from -78 deg C to room temp.

With thionyl chloride; In diethyl ether;