methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside
CAS No.:112255-06-8
Molecular Formula:C₂₈H₃₀O₃
Molecular Weight:414.544
Hs Code.:

Synonyms:methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

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Technology Process of methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

There total 3 articles about methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.6%

: 917-54-4
methyllithium

: 112255-17-1
methyl 2-O-acetyl-3,4-dideoxy-2-C-methyl-6-O-trityl-α-D-threo-hex-3-enopyranoside

: 112255-06-8
methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With copper(l) iodide; In diethyl ether; at -40 ℃; for 4h;
DOI:10.1246/bcsj.60.1441

Reference yield:

: 35303-94-7
(2S,6S)-2-Methoxy-6-trityloxymethyl-6H-pyran-3-one

: 112255-06-8
methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 4 h / -78 °C

2: pyridine, 4-dimethylamino pyridine

3: 82.6 percent / Cu(I)I / diethyl ether / 4 h / -40 °C

With pyridine; dmap; copper(l) iodide; In diethyl ether;
DOI:10.1246/bcsj.60.1441

Reference yield:

: 112255-16-0
(2S,3S,6S)-2-Methoxy-3-methyl-6-trityloxymethyl-3,6-dihydro-2H-pyran-3-ol

: 112255-06-8
methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, 4-dimethylamino pyridine

2: 82.6 percent / Cu(I)I / diethyl ether / 4 h / -40 °C

With pyridine; dmap; copper(l) iodide; In diethyl ether;
DOI:10.1246/bcsj.60.1441