CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

Base Information

Chemical Name:CoGe(C₆H₅)3P(OC₆H₅)3(CO)3
CAS No.:42989-54-8
Molecular Formula:C₃₉H₃₀CoGeO₆P
Molecular Weight:757.221
Hs Code.:

CoGe(C<sub>6</sub>H<sub>5</sub>)3P(OC<sub>6</sub>H<sub>5</sub>)3(CO)3

Synonyms:CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

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Chemical Property of CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

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Technology Process of CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

There total 1 articles about CoGe(C₆H₅)3P(OC₆H₅)3(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 21118-36-5,55449-52-0
Co₂(CO)6{P(O(C₆H₅))3}2

: 2816-43-5
triphenylgermane

: 42989-54-8
CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

Guidance literature:: In toluene; byproducts: H2; under N2 a mixt. of Co-complex and Ph3GeH was refluxed in toluene for 72 h; filtered, concd., n-pentane was added, stood at -20°C, crystd.; elem. anal.;
DOI:10.1016/S0022-328X(00)82934-4

Reference yield: 92.0%

: 16853-85-3
lithium aluminium tetrahydride

: 42989-54-8
CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

: 2816-43-5
triphenylgermane

Guidance literature:: With hydrogenchloride; In diethyl ether; under N2 a soln. of Co-complex in ether was stirred for 2 d at room temp. with excess of LiAlH4, hydrolysis with aq. HCl; chromd. (silica gel, hexane/benzene);
DOI:10.1016/S0022-328X(00)82934-4

Reference yield:

: 42989-54-8
CoGe(C₆H₅)3P(OC₆H₅)3(CO)3

: 1626-24-0
chlorotriphenylgermane

: 1613-66-7
dichlorodiphenylgermane

Guidance literature:: With aluminium trichloride; In diethyl ether; under N2 a soln. of Co-complex in ether was treated with AlCl3 for 8 d; monitored by IR, pumped off;
DOI:10.1016/S0022-328X(00)82934-4