p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

Base Information

Chemical Name:p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside
CAS No.:183878-41-3
Molecular Formula:C₁₄H₁₆ClNO₇
Molecular Weight:345.737
Hs Code.:

Synonyms:p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

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Technology Process of p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

There total 3 articles about p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (3aR,4S,6R,7S,7aS)-2-Ethoxy-2,4-dimethyl-6-(4-nitro-phenoxy)-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ol

: 183878-41-3
p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

Guidance literature:: With hydrogenchloride; In dichloromethane;
DOI:10.1002/(SICI)1521-3773(19991216)38:24<3680::AID-ANIE3680>3.0.CO;2-9

Reference yield:

: 22153-71-5
1-(4-nitrophenyl)-β-L-fucopyranoside

: 78-39-7
Triethyl orthoacetate

: 183878-41-3
p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

Guidance literature:: With hydrogenchloride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 22153-71-5
1-(4-nitrophenyl)-β-L-fucopyranoside

: 183878-41-3
p-nitrophenyl 3,6-dideoxy-3-chloro-4-O-acetyl-β-L-guloside

Guidance literature:: Multi-step reaction with 2 steps

1: p-TosOH / tetrahydrofuran

2: 70 percent / HCl / CH₂Cl₂

With hydrogenchloride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; 1: Cyclization / 2: Ring cleavage;
DOI:10.1002/(SICI)1521-3773(19991216)38:24<3680::AID-ANIE3680>3.0.CO;2-9