C₂₅H₂₆N₆O₅

Base Information

Chemical Name:C₂₅H₂₆N₆O₅
CAS No.:1527481-28-2
Molecular Formula:C₂₅H₂₆N₆O₅
Molecular Weight:490.519
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:C₂₅H₂₆N₆O₅

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Chemical Property of C₂₅H₂₆N₆O₅

Chemical Property:

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Technology Process of C₂₅H₂₆N₆O₅

There total 8 articles about C₂₅H₂₆N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 1527481-27-1
C₂₈H₃₂N₆O₅

: 1527481-28-2
C₂₅H₂₆N₆O₅

: 1527481-29-3
C₂₆H₂₈N₆O₅

Guidance literature:: With boron tribromide; In dichloromethane; at -78 - 20 ℃; Inert atmosphere; Darkness;
DOI:10.1016/j.tet.2013.11.060

Reference yield:

: 1011708-94-3
5-isopropyl-2,3,4-trimethoxybenzaldehyde

: 1527481-28-2
C₂₅H₂₆N₆O₅

: 1527481-29-3
C₂₆H₂₈N₆O₅

Guidance literature:: Multi-step reaction with 9 steps

1: tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: dmap; 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; acetone / 2 h / Inert atmosphere; Reflux

4: diisobutylaluminium hydride / dichloromethane; hexane / 2.5 h / -78 - -40 °C / Inert atmosphere

5: tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

7: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / chloroform; dimethyl sulfoxide / 2 h / Reflux

8: sodium L-ascorbate; copper(ll) sulfate pentahydrate / chloroform; water / 2 h / Inert atmosphere; Reflux

9: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere; Darkness

With 1H-imidazole; dmap; copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; boron tribromide; diisobutylaluminium hydride; sodium L-ascorbate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone;
DOI:10.1016/j.tet.2013.11.060

Reference yield:

: 1527481-03-3
C₁₅H₂₀O₄

: 1527481-28-2
C₂₅H₂₆N₆O₅

: 1527481-29-3
C₂₆H₂₈N₆O₅

Guidance literature:: Multi-step reaction with 8 steps

1: dmap; 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; acetone / 2 h / Inert atmosphere; Reflux

3: diisobutylaluminium hydride / dichloromethane; hexane / 2.5 h / -78 - -40 °C / Inert atmosphere

4: tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / chloroform; dimethyl sulfoxide / 2 h / Reflux

7: sodium L-ascorbate; copper(ll) sulfate pentahydrate / chloroform; water / 2 h / Inert atmosphere; Reflux

8: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere; Darkness

With 1H-imidazole; dmap; copper(ll) sulfate pentahydrate; tetrabutyl ammonium fluoride; boron tribromide; diisobutylaluminium hydride; sodium L-ascorbate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone;
DOI:10.1016/j.tet.2013.11.060