(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

Base Information

Chemical Name:(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine
CAS No.:439864-43-4
Molecular Formula:C₂₅H₃₂N₄O₇
Molecular Weight:500.552
Hs Code.:

(S)-N<sup>2</sup>-benzyloxycarbonyl-N<sup>6</sup>-tertbutoxycarbonyl-N<sup>4</sup>-phenylcarbamoyl-4-azalysine

Synonyms:(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

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Technology Process of (S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

There total 11 articles about (S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 439864-36-5
methyl (S)-N²-benzyloxycarbonyl-N⁶-tert-butoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysinate

: 439864-43-4
(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

Guidance literature:: With lithium hydroxide; In methanol; water; at 20 ℃;
DOI:10.1021/jo010456e

Reference yield:

: 2304-96-3
N-benzyloxycarbonyl-L-asparagine

: 439864-43-4
(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / iodosobenzene diacetate / ethyl acetate; acetonitrile; H₂O / 4.5 h / 15 - 20 °C

2: 78 percent / HCl / 5 °C

3: 65 percent / acetic acid; sodium cyanoborohydride / methanol

4: 69 percent / diethyl ether / 5 h / 20 °C

5: 98 percent / LiOH / H₂O; methanol / 20 °C

With hydrogenchloride; lithium hydroxide; [bis(acetoxy)iodo]benzene; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1021/jo010456e

Reference yield:

: 89711-08-0
N-(t-butoxycarbonyl)glycinal

: 439864-43-4
(S)-N²-benzyloxycarbonyl-N⁶-tertbutoxycarbonyl-N⁴-phenylcarbamoyl-4-azalysine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / acetic acid; sodium cyanoborohydride / methanol

2: 69 percent / diethyl ether / 5 h / 20 °C

3: 98 percent / LiOH / H₂O; methanol / 20 °C

With lithium hydroxide; sodium cyanoborohydride; acetic acid; In methanol; diethyl ether; water;
DOI:10.1021/jo010456e