Technology Process of C34H37NO4S
There total 4 articles about C34H37NO4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); ammonium formate;
In
toluene;
at 80 ℃;
for 0.666667h;
Inert atmosphere;
DOI:10.1021/ja302765m
- Guidance literature:
-
Multi-step reaction with 4 steps
1: perchloric acid / tetrahydrofuran; water / 4 h / 22 °C / Inert atmosphere
2: tetrahydrofuran; toluene / 0 - 60 °C / Inert atmosphere
3: dmap; triethylamine / dichloromethane / 0 - 40 °C / Inert atmosphere
4: tetrakis(triphenylphosphine) palladium(0); ammonium formate / toluene / 0.67 h / 80 °C / Inert atmosphere
With
dmap; tetrakis(triphenylphosphine) palladium(0); perchloric acid; ammonium formate; triethylamine;
In
tetrahydrofuran; dichloromethane; water; toluene;
4: Tsuji reduction;
DOI:10.1021/ja302765m
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran; toluene / 0 - 60 °C / Inert atmosphere
2: dmap; triethylamine / dichloromethane / 0 - 40 °C / Inert atmosphere
3: tetrakis(triphenylphosphine) palladium(0); ammonium formate / toluene / 0.67 h / 80 °C / Inert atmosphere
With
dmap; tetrakis(triphenylphosphine) palladium(0); ammonium formate; triethylamine;
In
tetrahydrofuran; dichloromethane; toluene;
3: Tsuji reduction;
DOI:10.1021/ja302765m
