4-octyl-2,6-bispyrazolylpyridine

Base Information

Chemical Name:4-octyl-2,6-bispyrazolylpyridine
CAS No.:1369968-56-8
Molecular Formula:C₇₂H₉₂N₁₀
Molecular Weight:1097.59
Hs Code.:

Synonyms:4-octyl-2,6-bispyrazolylpyridine

Suppliers and Price of 4-octyl-2,6-bispyrazolylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-octyl-2,6-bispyrazolylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-octyl-2,6-bispyrazolylpyridine

There total 7 articles about 4-octyl-2,6-bispyrazolylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 204923-11-5
[1,1',4',1'-terphenyl]-4,4'-diyldiboronic acid

: 1369968-48-8
4-iodo-2,6-bis(4-octyl-1H-pyrazol-1-yl)pyridine

: 1369968-56-8
4-octyl-2,6-bispyrazolylpyridine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; at 80 ℃; for 72h; Inert atmosphere;
DOI:10.1021/jo300050m

Reference yield:

: 1369968-45-5
ethyl 2,6-bis(4-octyl-1H-pyrazol-1-yl)isonicotinate

: 1369968-56-8
4-octyl-2,6-bispyrazolylpyridine

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hydroxide / tetrahydrofuran; water / 1 h

1.2: 1 h

2.1: oxalyl dichloride / tetrahydrofuran; dichloromethane / 4 h / 20 °C

3.1: sodium azide / water; acetone

4.1: benzene / 16 h / Reflux

5.1: potassium carbonate / methanol / 8 h

5.2: 2 h / Cooling with ice

6.1: iodine; potassium iodide; isopentyl nitrite / dichloromethane / 12 h / Inert atmosphere; Heating

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane / 72 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; oxalyl dichloride; iodine; sodium carbonate; potassium carbonate; potassium iodide; lithium hydroxide; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; benzene; 4.1: Curtius rearrangement / 7.1: Suzuki coupling;
DOI:10.1021/jo300050m

Reference yield:

: 1369968-46-6
2,6-bis(4-(octyl)-1-ynyl-1H-pyrazol-1-yl)isonicotinic acid

: 1369968-56-8
4-octyl-2,6-bispyrazolylpyridine

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride / tetrahydrofuran; dichloromethane / 4 h / 20 °C

2.1: sodium azide / water; acetone

3.1: benzene / 16 h / Reflux

4.1: potassium carbonate / methanol / 8 h

4.2: 2 h / Cooling with ice

5.1: iodine; potassium iodide; isopentyl nitrite / dichloromethane / 12 h / Inert atmosphere; Heating

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane / 72 h / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium azide; oxalyl dichloride; iodine; sodium carbonate; potassium carbonate; potassium iodide; isopentyl nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; benzene; 3.1: Curtius rearrangement / 6.1: Suzuki coupling;
DOI:10.1021/jo300050m