Methyl 2-iodobenzyl sulfide

Base Information

• Chemical Name: Methyl 2-iodobenzyl sulfide
• CAS No.: 117760-02-8
• Molecular Formula: C₈H₉IS
• Molecular Weight: 264.13

Synonyms:Methyl 2-iodobenzyl sulfide

Chemical Property of Methyl 2-iodobenzyl sulfide

Chemical Property:

Purity/Quality:

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Technology Process of Methyl 2-iodobenzyl sulfide

There total 1 articles about Methyl 2-iodobenzyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-(2-iodo-benzyl)-isothiourea + dimethyl sulfate (77-78-1) → Methyl 2-iodobenzyl sulfide (117760-02-8)

Guidance literature:

With sodium hydroxide; In water; at 105 ℃; for 2h;

Reference yield: 100.0%

Thien-3-ylboronic acid (6165-69-1) + Methyl 2-iodobenzyl sulfide (117760-02-8) → C12H12S2

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 3h; Heating / reflux;

Reference yield: 100.0%

benzo[b]thiophene-2-boronic acid (98437-23-1) + Methyl 2-iodobenzyl sulfide (117760-02-8) → C16H14S2

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; for 3h; Heating / reflux;

upstream raw materials:

dimethyl sulfate

Downstream raw materials:

2-MeSCH₂C₆H₄CH₂B(OCMe₂)2

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