C₅₈H₈₂N₈O₄

Base Information

Chemical Name:C₅₈H₈₂N₈O₄
CAS No.:1246523-19-2
Molecular Formula:C₅₈H₈₂N₈O₄
Molecular Weight:955.34
Hs Code.:

C<sub>58</sub>H<sub>82</sub>N<sub>8</sub>O<sub>4</sub>

Synonyms:C₅₈H₈₂N₈O₄

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Chemical Property of C₅₈H₈₂N₈O₄

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Technology Process of C₅₈H₈₂N₈O₄

There total 8 articles about C₅₈H₈₂N₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1246523-16-9
C₃₄H₅₈O₄

: 70483-81-7
2-amino-4-benzyloxy-6-methylpyrimidine

: 1246523-19-2
C₅₈H₈₂N₈O₄

Guidance literature:: C₃₄H₅₈O₄; With diphenyl phosphoryl azide; triethylamine; at 25 - 60 ℃; for 4h; Inert atmosphere;

2-amino-4-benzyloxy-6-methylpyrimidine; for 20h; Inert atmosphere; Reflux;
DOI:10.1021/ma101647j

Reference yield:

: 1246523-04-5
C₁₃H₂₄Br₂

: 1246523-19-2
C₅₈H₈₂N₈O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 25 °C / Inert atmosphere

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 15 h / 25 °C / Inert atmosphere

3.1: hydrogen; palladium / tetrahydrofuran; ethanol / 20 h / 25 °C / 760.05 Torr / Inert atmosphere

4.1: potassium hydroxide / tetrahydrofuran; methanol; water / 18 h / Inert atmosphere; Reflux

5.1: diphenyl phosphoryl azide; triethylamine / 4 h / 25 - 60 °C / Inert atmosphere

5.2: 20 h / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; diphenyl phosphoryl azide; hydrogen; palladium; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/ma101647j

Reference yield:

: 1246523-07-8
C₁₃H₂₄

: 1246523-19-2
C₅₈H₈₂N₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran; N,N-dimethyl-formamide / 15 h / 25 °C / Inert atmosphere

2.1: hydrogen; palladium / tetrahydrofuran; ethanol / 20 h / 25 °C / 760.05 Torr / Inert atmosphere

3.1: potassium hydroxide / tetrahydrofuran; methanol; water / 18 h / Inert atmosphere; Reflux

4.1: diphenyl phosphoryl azide; triethylamine / 4 h / 25 - 60 °C / Inert atmosphere

4.2: 20 h / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diphenyl phosphoryl azide; hydrogen; palladium; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ma101647j