C₃₁H₄₃ClO₇Si

Base Information

Chemical Name:C₃₁H₄₃ClO₇Si
CAS No.:1332271-63-2
Molecular Formula:C₃₁H₄₃ClO₇Si
Molecular Weight:591.217
Hs Code.:

C<sub>31</sub>H<sub>43</sub>ClO<sub>7</sub>Si

Synonyms:C₃₁H₄₃ClO₇Si

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Chemical Property of C₃₁H₄₃ClO₇Si

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Technology Process of C₃₁H₄₃ClO₇Si

There total 1 articles about C₃₁H₄₃ClO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₃₁H₄₅ClO₇Si

: 1332271-63-2
C₃₁H₄₃ClO₇Si

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield: 81.0%

: 1332271-63-2
C₃₁H₄₃ClO₇Si

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1332271-25-6
C₃₇H₅₇ClO₈Si₂

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 40h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1332271-63-2
C₃₁H₄₃ClO₇Si

: 1332271-33-6
C₄₇H₅₉ClO₁₃Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

5.1: chromium dichloride; nickel dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

6.1: pyridine; Dess-Martin periodane / dichloromethane / 4.5 h / 20 °C / Inert atmosphere

7.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.5 h / 0 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 70 °C / Inert atmosphere

9.1: 2,6-dimethylpyridine / dichloromethane / 2.55 h / -78 - -45 °C / Inert atmosphere

10.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 14 h / 20 °C / Inert atmosphere

11.1: pyridinium p-toluenesulfonate / methanol / 16 h / 35 °C / Inert atmosphere

12.1: dmap; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 3 h / 0 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; chromium dichloride; dmap; sodium tetrahydroborate; osmium(VIII) oxide; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; Dess-Martin periodane; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; nickel dichloride; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol; 5.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1016/j.tet.2011.04.094