(4aZ,8aZ,12aZ,16aZ)-tetraphenylene

Base Information

Chemical Name:(4aZ,8aZ,12aZ,16aZ)-tetraphenylene
CAS No.:212-74-8
Molecular Formula:C24H16
Molecular Weight:304.391
Hs Code.:
Wikidata:Q82983699
Metabolomics Workbench ID:54834
Mol file:212-74-8.mol

Synonyms:CHEBI:33149;(4aZ,8aZ,12aZ,16aZ)-tetraphenylene

Suppliers and Price of (4aZ,8aZ,12aZ,16aZ)-tetraphenylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (4aZ,8aZ,12aZ,16aZ)-tetraphenylene

Chemical Property:

Vapor Pressure:9.72E-13mmHg at 25°C
Melting Point:232-235 °C(lit.)
Refractive Index:1.757
Boiling Point:577.6°Cat760mmHg
Flash Point:297.9°C
PSA：0.00000
Density:1.19g/cm³
LogP:5.14800
XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:304.125200510
Heavy Atom Count:24
Complexity:762

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C=CC=CC3=C4C=CC=CC4=C5C=CC=CC5=C2C=C1
Isomeric SMILES:C1=C/C/2=C\3/C(=C/4\C(=C\5/C(=C2/C=C1)/C=CC=C5)\C=CC=C4)/C=CC=C3

Technology Process of (4aZ,8aZ,12aZ,16aZ)-tetraphenylene

There total 12 articles about (4aZ,8aZ,12aZ,16aZ)-tetraphenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2236-52-4
2,2'-diiodobiphenyl

: 259-79-0
bisbenzocyclobutene

: 212-74-8
tetraphenylene

Guidance literature:: With n-butyllithium; copper dichloride; zinc(II) chloride; In tetrahydrofuran; hexane; 1.) -78 deg C; 2.) - 50 deg C; 3.) -78 deg C, 2 h then RT;
DOI:10.1016/S0040-4039(98)01082-X

Reference yield: 80.0%

: 13029-09-9
2,2'-dibromobiphenyl

: 259-79-0
bisbenzocyclobutene

: 212-74-8
tetraphenylene

Guidance literature:: With n-butyllithium; copper dichloride; zinc(II) chloride; In tetrahydrofuran; hexane; 1.) -78 deg C; 2.) - 50 deg C; 3.) -78 deg C, 2 h then RT;
DOI:10.1016/S0040-4039(98)01082-X

Reference yield: 68.0%

: 2113-51-1
2-iodobiphenyl

: 92-52-4,1594-86-1
biphenyl

: 212-74-8
tetraphenylene

Guidance literature:: With palladium diacetate; silver carbonate; trifluoroacetic acid; at 100 ℃; for 12h; Reagent/catalyst;
DOI:10.1021/acs.orglett.6b00641