((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2

Base Information

• Chemical Name: ((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2
• CAS No.: 1017968-11-4
• Molecular Formula: C₉₉H₁₄₇N₅O₃₇
• Molecular Weight: 1999.27

Synonyms:((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2

Chemical Property of ((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2

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Technology Process of ((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2

There total 1 articles about ((HO)2C₆H₃C(O)NH(CH₂)3)3CC(O)NH(CH₂)4NHC(O)C₆H₃(OCH₂C₆H₂(O(CH₂CH₂O)3CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C117H171N5O37 (1017968-12-5) → ((HO)2C6H3C(O)NH(CH2)3)3CC(O)NH(CH2)4NHC(O)C6H3(OCH2C6H2(O(CH2CH2O)3CH3)3)2 (1017968-11-4)

Guidance literature:

C₁₁₇H₁₇₁N₅O₃₇; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 1h; Inert atmosphere;

With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/b9nj00305c

Reference yield:

sodium [99Tc]pertechnetate (13718-28-0,65146-78-3,131626-77-2,34316-43-3) + ((HO)2C6H3C(O)NH(CH2)3)3CC(O)NH(CH2)4NHC(O)C6H3(OCH2C6H2(O(CH2CH2O)3CH3)3)2 (1017968-11-4) → (99)Tc((O2C6H3C(O)NH(CH2)3)3CC(O)NH(CH2)4NHC(O)C6H3(OCH2C6H2(O(CH2CH2O)3CH3)3)2)

Guidance literature:

With stannous chloride; NaOH; sodium ascorbate; In H₂O; aq. HCl; under Ar; ligand dissolved in H2O; soln. of Sn compd. in aq. HCl added; Na(99)TcO4 soln. added; aq. NaOH and aq. Na ascorbate added (pH ca. 7); stirred at room temp. for 15 min; stored for 45 min; detd. by thin layer chromy.;

DOI:10.1039/b9nj00305c

upstream raw materials:

C₁₁₇H₁₇₁N₅O₃₇

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