(10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

Base Information

Chemical Name:(10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)
CAS No.:402505-34-4
Molecular Formula:C₅₂H₄₈N₄O₄Zn
Molecular Weight:858.368
Hs Code.:

Synonyms:(10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

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Chemical Property of (10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

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Technology Process of (10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

There total 1 articles about (10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 402505-25-3
(5-bromo-10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)

: 536-74-3
phenylacetylene

: 402505-34-4
(10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

Guidance literature:: With As(C₆H₅)3; (C₂H₅)3N; Pd₂(C₆H₅CHCHCOCHCHC₆H₅)3; In tetrahydrofuran; triethylamine; under N2; Zn complex, ethynylbenzene, Pd complex and As(C6H5)3 were dissolved in THF/triethylamine (5/1), mixt. was stirred for 14 h at 40°C; solvent was evapd., residue was chromd. (silica gel, hexanes/THF (3/1));
DOI:10.1021/ja012489h

Reference yield: 99.0%

: 2396-63-6
hepta-1,6-diyne

: 402505-34-4
(10,20-bis[4-(3-methoxy-3-methylbutoxy)phenyl]-5-(phenylethynyl)porphinato)zinc(II)

: 402505-35-5
5-phenyl-6-[(5'-10',20'-bis[4-(3-methoxy-3-methylbutoxy)phenyl]porphinato)zinc(II)]indane

Guidance literature:: With Co₂(CO)8; In 1,4-dioxane; toluene; under N2; Zn complex and Co2(CO)8 were dissolved in toluene/dioxane (4/1) and heated to 100°C, a soln. of 1,6-heptadiyne in toluene was added dropwise (90 min); soln. was evapd. to dryness, residue was chromd. (silica gel, hexanes/THF (4/1));
DOI:10.1021/ja012489h