6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

Base Information

Chemical Name:6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose
CAS No.:154796-66-4
Molecular Formula:C₂₈H₃₈O₆Si
Molecular Weight:498.692
Hs Code.:

Synonyms:6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

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Chemical Property of 6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

Chemical Property:

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Technology Process of 6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

There total 5 articles about 6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 155809-03-3
6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-D-mannose diethyl dithioacetal

: 154796-66-4
6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

Guidance literature:: With water; mercury dichloride; mercury(II) oxide; In dichloromethane; acetonitrile; for 0.5h; Ambient temperature;

Reference yield:

: 6748-69-2
D-mannose diethyl dithioacetal

: 154796-66-4
6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

Guidance literature:: Multi-step reaction with 3 steps

1: TEA / dimethylformamide / 1 h / Ambient temperature

2: 10-camphorsulphonic acid (CSA) / 6 h / Ambient temperature

3: 95 percent / H₂O, HgO, HgCl₂ / CH₂Cl₂; acetonitrile / 0.5 h / Ambient temperature

With TEA; camphor-10-sulfonic acid; water; mercury dichloride; mercury(II) oxide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: (2S,3S,4R,5R)-6-(tert-Butyl-diphenyl-silanyloxy)-1,1-bis-ethylsulfanyl-hexane-2,3,4,5-tetraol

: 154796-66-4
6-(O-tert-butyldiphenylsilyl)-2,4:3,5-di-O-isopropylidene-aldehydo-D-mannose

Guidance literature:: Multi-step reaction with 2 steps

1: 10-camphorsulphonic acid (CSA) / 6 h / Ambient temperature

2: 95 percent / H₂O, HgO, HgCl₂ / CH₂Cl₂; acetonitrile / 0.5 h / Ambient temperature

With camphor-10-sulfonic acid; water; mercury dichloride; mercury(II) oxide; In dichloromethane; acetonitrile;