4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

Base Information

Chemical Name:4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin
CAS No.:119882-24-5
Molecular Formula:C₁₅H₁₄N₂S₂
Molecular Weight:286.422
Hs Code.:

Synonyms:4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

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Technology Process of 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

There total 3 articles about 4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 119882-35-8
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-nitrobenzen

: 119882-24-5
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

Guidance literature:: With sodium dithionite; sodium carbonate; In 1,4-dioxane; water; at 50 ℃;

Reference yield:

: 555-21-5,34512-13-5,174848-08-9
4-Nitrophenylacetonitrile

: 119882-24-5
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NEt₃ / propan-1-ol / 1 h / Heating

2: 36 percent / Na₂S₂O₄, Na₂CO₃ / H₂O; dioxane / 50 °C

With sodium dithionite; sodium carbonate; triethylamine; In 1,4-dioxane; propan-1-ol; water;

Reference yield:

: 59102-97-5
2-Methylthio-4,5-tetramethylen-1,3-dithiolium-iodid

: 119882-24-5
4-<α-(4,5-Tetramethylen-(2H)1,3-dithiol-2-yliden)-α-cyanomethyl>-anilin

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NEt₃ / propan-1-ol / 1 h / Heating

2: 36 percent / Na₂S₂O₄, Na₂CO₃ / H₂O; dioxane / 50 °C

With sodium dithionite; sodium carbonate; triethylamine; In 1,4-dioxane; propan-1-ol; water;