C₃₁H₃₂Cl₄O₆

Base Information

Chemical Name:C₃₁H₃₂Cl₄O₆
CAS No.:936338-09-9
Molecular Formula:C₃₁H₃₂Cl₄O₆
Molecular Weight:642.403
Hs Code.:

C<sub>31</sub>H<sub>32</sub>Cl<sub>4</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₂Cl₄O₆

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Chemical Property of C₃₁H₃₂Cl₄O₆

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Technology Process of C₃₁H₃₂Cl₄O₆

There total 11 articles about C₃₁H₃₂Cl₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₂Cl₄O₄

: 936338-09-9
C₃₁H₃₂Cl₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: (PCy₃)2Ru=CHPh / CH₂Cl₂ / 5 h / Heating

2.1: 3.50 g / lead(IV) acetate / CH₂Cl₂ / 20 °C

3.1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

4.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

5.1: florisil / CH₂Cl₂ / 2 h

6.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

7.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

8.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

9.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

10.1: CH₂Cl₂ / 3 h / 35 °C

10.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With lead(IV) acetate; florisil; n-butyllithium; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; (PCy₃)2Ru=CHPh; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: 936338-30-6
C₂₆H₂₆Cl₄O₄

: 936338-09-9
C₃₁H₃₂Cl₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

2.1: florisil / CH₂Cl₂ / 2 h

3.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

4.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

5.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

6.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

7.1: CH₂Cl₂ / 3 h / 35 °C

7.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With florisil; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: C₂₆H₂₆Cl₄O₄

: 936338-09-9
C₃₁H₃₂Cl₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

2.1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

3.1: florisil / CH₂Cl₂ / 2 h

4.1: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

5.1: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

6.1: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

7.1: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

8.1: CH₂Cl₂ / 3 h / 35 °C

8.2: 356 mg / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 1 h / 20 °C

With florisil; n-butyllithium; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474