1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene

Base Information

Chemical Name:1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene
CAS No.:110931-87-8
Molecular Formula:C₁₅H₁₇BrSi
Molecular Weight:305.289
Hs Code.:
DSSTox Substance ID:DTXSID401245687

Synonyms:1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene;SCHEMBL9694603;DTXSID401245687;110931-87-8

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:304.02829
Heavy Atom Count:17
Complexity:225

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C1=CC=CC=C1)C2=CC=C(C=C2)CBr

Technology Process of 1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene

There total 4 articles about 1-(Bromomethyl)-4-(dimethylphenylsilyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 110931-88-9
Dimethyl-(4-methylphenyl)-phenylsilan

: 110931-87-8
(4-Brommethylphenyl)-dimethylphenylsilan

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 9h; Heating;
DOI:10.1002/ardp.19933260608

Reference yield:

: 106-38-7
para-bromotoluene

: 110931-87-8
(4-Brommethylphenyl)-dimethylphenylsilan

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-BuLi / 1) THF, -65 deg C, 30 min, 2) warmup to room temperature, then room temperature, 2 h

2: 85 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 9 h / Heating

With N-Bromosuccinimide; n-butyllithium; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1002/ardp.19933260608

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 110931-87-8
(4-Brommethylphenyl)-dimethylphenylsilan

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-BuLi / 1) THF, -65 deg C, 30 min, 2) warmup to room temperature, then room temperature, 2 h

2: 85 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 9 h / Heating

With N-Bromosuccinimide; n-butyllithium; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1002/ardp.19933260608