(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

Base Information

Chemical Name:(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol
CAS No.:1123178-76-6
Molecular Formula:C₆₅H₇₅NO₂₆
Molecular Weight:1286.3
Hs Code.:

(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

Synonyms:(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

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Chemical Property of (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

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Technology Process of (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

There total 1 articles about (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1123178-74-4
(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-D-lyxo-hexitol

: 111437-25-3
benzyl (R)-(+)-3-phenyl-2-(trifluoromethylsulfonyloxy)propanoate

: 1123178-76-6
(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

Guidance literature:: (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-D-lyxo-hexitol; With di(n-butyl)tin oxide; In benzene; at 80 ℃; for 3h; Inert atmosphere;

benzyl (R)-(+)-3-phenyl-2-(trifluoromethylsulfonyloxy)propanoate; With cesium fluoride; In 1,2-dimethoxyethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/jm801058n

Reference yield: 76.0%

: 1123178-76-6
(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol

: (sodium 5-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-β-D-galactopyranosyl-(1->3)-1,5-anhydro-2-deoxy-6-O-[sodium (S)-1-carboxylato-2-phenyl-ethyl]-D-lyxo-hexitol

Guidance literature:: (benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosynate)-(2->3)-(2,4-di-O-acetyl-6-O-benzoyl-β-D-galactopyranosyl)-(1->3)-1,5-anhydro-2-deoxy-6-O-[(S)-1-benzoxycarbonyl-2-benzyl-ethyl]-D-lyxo-hexitol; With methanol; sodium methylate; at 20 ℃; for 21h; Inert atmosphere;

With water; In methanol; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm801058n