3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide

Base Information

• Chemical Name: 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide
• CAS No.: 1055899-91-6
• Molecular Formula: C₂₇H₃₄N₂O₃S₂
• Molecular Weight: 498.711

Synonyms:3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide

Chemical Property of 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide

Chemical Property:

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Technology Process of 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide

There total 1 articles about 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-oxycarbonylmethylphenyl)-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide (697746-49-9) + benzylamine (100-46-9) → 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide (1055899-91-6)

Guidance literature:

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1016/j.bmc.2007.07.026

Reference yield:

3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide (1055899-91-6) → 3-[4-(N-benzylcarbamoylmethyl)phenyl]-5-iso-butylthiophene-2-sulfonamide

Guidance literature:

With trifluoroacetic acid; In methoxybenzene; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2007.07.026

upstream raw materials:

3-(4-oxycarbonylmethylphenyl)-5-iso-butyl-N-tert-butylthiophene-2-sulfonamide

benzylamine

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