Technology Process of C62H62O2P2(2+)
There total 6 articles about C62H62O2P2(2+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 24 h / 70 °C / Reflux
2.1: sodium acetate / acetic acid / 14 h / Reflux
3.1: sodium hydroxide / methanol; water / 17 h / Reflux
4.1: tetrabutylammomium bromide; sodium dithionite / water; tetrahydrofuran / 0.17 h / 20 °C
4.2: 30 h / Reflux
5.1: thionyl chloride / chloroform / 3 h / 5 - 20 °C
6.1: toluene / 24 h / Reflux
With
N-Bromosuccinimide; thionyl chloride; sodium dithionite; tetrabutylammomium bromide; sodium acetate; sodium hydroxide; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; chloroform; water; acetic acid; toluene;
DOI:10.1039/c2cp42512b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutylammomium bromide; sodium dithionite / water; tetrahydrofuran / 0.17 h / 20 °C
1.2: 30 h / Reflux
2.1: thionyl chloride / chloroform / 3 h / 5 - 20 °C
3.1: toluene / 24 h / Reflux
With
thionyl chloride; sodium dithionite; tetrabutylammomium bromide;
In
tetrahydrofuran; chloroform; water; toluene;
DOI:10.1039/c2cp42512b