2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

Base Information

• Chemical Name: 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide
• CAS No.: 18311-30-3
• Molecular Formula: C₆₁H₄₉BrO₁₇
• Molecular Weight: 1133.95

Synonyms:2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

Chemical Property of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

Chemical Property:

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Technology Process of 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide

There total 2 articles about 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-(1,2,3,6-tetra-O-benzoyl)-β-D-glucopyranose (4710-82-1) → 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide (18311-30-3)

Guidance literature:

With hydrogen bromide; acetic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/acs.orglett.7b02760

Reference yield:

octabenzoyl-D-maltose (18311-29-0) → 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide (18311-30-3)

Guidance literature:

With hydrogen bromide; acetic acid; In dichloromethane; at 4 ℃;

DOI:10.1248/cpb.52.965

Reference yield: 89.0%

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl bromide (18311-30-3) → 2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol (75414-17-4)

Guidance literature:

With diethylamine; sodium iodide; In acetone; for 16h; Ambient temperature;

DOI:10.1021/jo00219a017

upstream raw materials:

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1→4)-(1,2,3,6-tetra-O-benzoyl)-β-D-glucopyranose

octabenzoyl-D-maltose

Downstream raw materials:

2,3,6-tri-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,5-anhydro-D-arabino-hex-1-enitol

2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->4)-2,3,6-tri-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate

3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-α-D-arabino-hexopyranos-2-ulosyl bromide

3,6-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1,5-anhydro-D-fructose oxime

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