phenyl-acetic acid-(methyl-nitroso-amide)

Base Information

• Chemical Name: phenyl-acetic acid-(methyl-nitroso-amide)
• CAS No.: 68782-25-2
• Molecular Formula: C₉H₁₀N₂O₂
• Molecular Weight: 178.191

Synonyms:phenyl-acetic acid-(methyl-nitroso-amide)

Chemical Property of phenyl-acetic acid-(methyl-nitroso-amide)

Chemical Property:

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Technology Process of phenyl-acetic acid-(methyl-nitroso-amide)

There total 2 articles about phenyl-acetic acid-(methyl-nitroso-amide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylphenylacetamide (6830-82-6) → phenyl-acetic acid-(methyl-nitroso-amide) (68782-25-2)

Guidance literature:

With potassium acetate; acetic anhydride; acetic acid; nitrosylchloride; weiteres Reagens: Phosphor(V)-oxid;

Reference yield:

→ phenyl-acetic acid-(methyl-nitroso-amide) (68782-25-2)

Guidance literature:

aus d. entspr. N-Methylamid;

DOI:10.1021/jo01319a046

Reference yield: 65.0%

phenyl-acetic acid-(methyl-nitroso-amide) (68782-25-2) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 1-(1H-indazol-1-yl)-2-phenylethan-1-one

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/d1cc05655g

upstream raw materials:

N-methylphenylacetamide

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