(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

Base Information

Chemical Name:(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid
CAS No.:131938-96-0
Molecular Formula:C₁₇H₁₇NO₄
Molecular Weight:299.326
Hs Code.:

Synonyms:(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

Chemical Property:

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Technology Process of (1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

There total 1 articles about (1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 133725-55-0
(2S,3S)-5-methyl-3-(1-tosylindol-3-yl)cyclohex-4-ene-1,2-dicarboxylic acid anhydride

: 131938-96-0
(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

Guidance literature:: With potassium hydroxide; In methanol; water; for 1h; Heating;

Reference yield:

: 131938-96-0
(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

: 131938-81-3
methyl 9-methyl-6-oxo-5-tosly-5,6,6aβ,7β,8,10aβ-hexahydroindeno<2,1-b>indole-7-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / BF₃*MeOH / 1 h / Heating

2: 68 percent / PPE / CHCl₃ / 0.5 h / Heating

3: 1) TBAHS, aq. NaOH / 1) benzene, RT, 5 min, 2) benzene

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; boron trifluoride methanol complex; In chloroform;

Reference yield:

: 131938-96-0
(1RS,2SR,3SR)-3-(indol-3'-yl)-5-methylcyclohex-4-ene-1,2-dicarboxylic acid

: 131939-00-9
(1RS,2SR,3SR)-2-methyl hydrogen 3-(indol-3'-yl)-5-methyl-cyclohex-4-ene-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 16 percent / BF₃*MeOH / 1 h / Heating

2: 52 percent / 3M KOH, tetrabutylammonium hydrogen sulphate / tetrahydrofuran / 2 h / Heating

With potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; boron trifluoride methanol complex; In tetrahydrofuran;