potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate

Base Information

• Chemical Name: potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate
• CAS No.: 205993-24-4
• Molecular Formula: C₂₉H₄₁N₂*K
• Molecular Weight: 456.756

Synonyms:potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate

Chemical Property of potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate

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Technology Process of potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate

There total 3 articles about potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) → potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate (205993-24-4)

Guidance literature:

With potassium hexamethylsilazane; In diethyl ether; at 20 ℃; for 18h;

DOI:10.1021/om3010965

Reference yield: 36.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) → HC(CMeN-2,6-i-Pr2C6H3)2K (205993-24-4)

Guidance literature:

With potassium hydride; In tetrahydrofuran; at 80 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1039/d0dt01342k

Reference yield:

[MgI(OEt2)(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-enyl)] (365999-36-6) → (κ2-{2,6-iPr2C6H3NCMe}2CH)Mg-Mg(κ2-{2,6-iPr2C6H3NCMe}2CH) (1005756-54-6) + potassium N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diiminate (205993-24-4)

Guidance literature:

With KC₈; In toluene; Inert atmosphere;

DOI:10.1002/chem.200902425

upstream raw materials:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

[MgI(OEt₂)(2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-enyl)]

Downstream raw materials:

[(CH(CH₃)2)2C₆H₃NCCH₃]2CHMnIC₄H₈O

(HC(CMeN-2,6-i-Pr2C6H3)2)(μ-Cl)2Mn(THF)2(μ-Cl)2Mn(HC(CMeN-2,6-i-Pr2C6H3)2)

Bi((N(C₆H₃(CH(CH₃)2)2)C(CH₃))2CH)(CF₃SO₃)2

(2,4-bis(2,6-diisopropylphenylimino)pentan-3-ide-.kappa2N,N')aluminum(I)

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