C₅₃H₃₆I₄

Base Information

Chemical Name:C₅₃H₃₆I₄
CAS No.:1267662-21-4
Molecular Formula:C₅₃H₃₆I₄
Molecular Weight:1180.49
Hs Code.:

C<sub>53</sub>H<sub>36</sub>I<sub>4</sub>

Synonyms:C₅₃H₃₆I₄

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Chemical Property of C₅₃H₃₆I₄

Chemical Property:

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Technology Process of C₅₃H₃₆I₄

There total 5 articles about C₅₃H₃₆I₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1267662-20-3
C₆₅H₇₂Si₄

: 1267662-21-4
C₅₃H₃₆I₄

Guidance literature:: With Iodine monochloride; In dichloromethane; at 0 ℃; for 12.5h; Inert atmosphere;
DOI:10.1002/chem.201002574

Reference yield:

: 934282-30-1
C₁₀H₁₇BO₂Si

: 1267662-21-4
C₅₃H₃₆I₄

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 1 h / Inert atmosphere; Reflux

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

3: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Iodine monochloride; sodium hydrogencarbonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1002/chem.201002574

Reference yield:

: 315668-55-4
3-bromo-5-trimethysilyltoluene

: 1267662-21-4
C₅₃H₃₆I₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.17 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dichloromethane / 1 h / Inert atmosphere; Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / Inert atmosphere; Reflux

4.1: Iodine monochloride / dichloromethane / 12.5 h / 0 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; Iodine monochloride; sodium hydrogencarbonate; In tetrahydrofuran; hexane; dichloromethane; water;
DOI:10.1002/chem.201002574