N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine

Base Information

• Chemical Name: N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine
• CAS No.: 1252003-60-3
• Molecular Formula: C₁₄H₁₉N₅S
• Molecular Weight: 289.404
• Mol file: 1252003-60-3.mol

Synonyms:N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine

Chemical Property of N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine

There total 2 articles about N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-cyclohexylidene-1-hydrazinecarboximidamide (4364-74-3) + phenyl isothiocyanate (103-72-0) → N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine (1252003-60-3)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 0.833333h;

DOI:10.1080/10426500903329237

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → N-(cyclohexylideneamino)-N'-(phenylthiocarbamoyl)guanidine (1252003-60-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / dimethyl sulfoxide / 1 h / 20 °C

2: dimethyl sulfoxide / 1 h

With sodium hydroxide; In dimethyl sulfoxide;

DOI:10.1016/j.tetlet.2014.08.033

upstream raw materials:

2-cyclohexylidene-1-hydrazinecarboximidamide

phenyl isothiocyanate

cyclohexanone