N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

Base Information

Chemical Name:N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide
CAS No.:1092459-39-6
Molecular Formula:C₁₅H₁₃F₃N₄O₂S
Molecular Weight:370.355
Hs Code.:

Synonyms:N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

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Chemical Property of N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

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Technology Process of N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

There total 5 articles about N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 210113-64-7
N-(4iodobenzyl)methanesulfonamide

: 1092459-55-6
3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridine

: 1092459-39-6
N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

Guidance literature:: With potassium carbonate; copper(l) iodide; dimethylaminoacetic acid; In dimethyl sulfoxide; at 190 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 1060802-29-0
C₇H₃BrF₃NO

: 1092459-39-6
N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; hydrazine / ethanol / 0.5 h / 120 °C

2: potassium carbonate / copper(l) iodide; dimethylaminoacetic acid / dimethyl sulfoxide / 0.5 h / 190 °C / Microwave irradiation

With hydrogenchloride; potassium carbonate; hydrazine; copper(l) iodide; dimethylaminoacetic acid; In ethanol; dimethyl sulfoxide;

Reference yield:

: 1092459-54-5
1-(3-bromo-4-pyridinyl)-2,2,2-trifluoroethanol

: 1092459-39-6
N-({4-[3-(trifluoromethyl)-1H-pyrazolo[3,4-c]pyridin-1-yl]phenyl}methyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 0.92 h / 100 °C / Microwave irradiation

2: hydrogenchloride; hydrazine / ethanol / 0.5 h / 120 °C

3: potassium carbonate / copper(l) iodide; dimethylaminoacetic acid / dimethyl sulfoxide / 0.5 h / 190 °C / Microwave irradiation

With hydrogenchloride; potassium carbonate; hydrazine; copper(l) iodide; dimethylaminoacetic acid; In ethanol; dichloromethane; dimethyl sulfoxide;