Technology Process of 5-(3-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid phenylamide
There total 7 articles about 5-(3-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid phenylamide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
TEA; hydrogen sulfide;
In
pyridine;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 68 percent / NaBH4 / methanol
2: 85 percent / H2 / Raney-Ni / methanol / 760 Torr
3: 1.) HCl/NaNO2 / 1.) H2O; 2.) 0-5 deg C 30 min, room temp. 4 h
4: PBr3 / CHCl3 / 1.5 h / Heating
5: C2H2ONa / ethanol / 5 h / Heating
7: 97 percent / TEA, H2S / pyridine / Ambient temperature
With
hydrogenchloride; sodium tetrahydroborate; C2H2ONa; TEA; hydrogen sulfide; hydrogen; phosphorus tribromide; sodium nitrite;
nickel;
In
pyridine; methanol; ethanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 85 percent / H2 / Raney-Ni / methanol / 760 Torr
2: 1.) HCl/NaNO2 / 1.) H2O; 2.) 0-5 deg C 30 min, room temp. 4 h
3: PBr3 / CHCl3 / 1.5 h / Heating
4: C2H2ONa / ethanol / 5 h / Heating
6: 97 percent / TEA, H2S / pyridine / Ambient temperature
With
hydrogenchloride; C2H2ONa; TEA; hydrogen sulfide; hydrogen; phosphorus tribromide; sodium nitrite;
nickel;
In
pyridine; methanol; ethanol; chloroform;
