N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

Base Information

Chemical Name:N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide
CAS No.:25829-00-9
Molecular Formula:C₁₉H₂₀BrNO₅
Molecular Weight:422.276
Hs Code.:

Synonyms:N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

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Chemical Property of N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

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Technology Process of N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

There total 9 articles about N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 4697-62-5
6-bromohomoveratric acid

: 1484-85-1
3,4-methylenedioxyphenylethylamine

: 25829-00-9
N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2019.130814

Reference yield: 80.0%

: 4697-62-5
6-bromohomoveratric acid

: 1653-64-1
homopiperonylamine hydrochloride

: 25829-00-9
N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

Guidance literature:: 6-bromohomoveratric acid; With thionyl chloride; at 76 ℃; for 1.5h;

homopiperonylamine hydrochloride; In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 25829-00-9
N-(2-(benzo[d] [1,3]dioxol-5-yl)ethyl)-2-(2-bromo-4,5-dimethoxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine

2: acetic acid; benzene; aqueous nitrous acid

With bromine; cis-nitrous acid; acetic acid; benzene;