6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

Base Information

Chemical Name:6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid
CAS No.:1447829-11-9
Molecular Formula:C₁₅H₁₉BrO₃
Molecular Weight:327.218
Hs Code.:

Synonyms:6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

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Chemical Property of 6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

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Technology Process of 6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

There total 11 articles about 6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1628293-34-4
C₂₀H₃₀BBrO₃

: 14660-45-8
potassium monomethylcarbonate

: 1447829-11-9
6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

Guidance literature:: With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1055/s-0033-1339119

Reference yield: 64.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1447829-16-4
C₂₀H₃₀BBrO₃

: 1447829-11-9
6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

Guidance literature:: carbon dioxide; C₂₀H₃₀BBrO₃; With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium tert-butylate; In tetrahydrofuran; at 70 ℃; for 16h; Inert atmosphere; Sealed tube;

With hydrogenchloride; In tetrahydrofuran; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/ol4019375

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 7-((4-bromobenzyl)oxy)hept-1-en-3-ol

: 1447829-11-9
6-((4-bromobenzyl)oxy)-2-vinylhexanoic acid

Guidance literature:: carbon dioxide; 7-((4-bromobenzyl)oxy)hept-1-en-3-ol; With diethylzinc; triphenylphosphine; palladium dichloride; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 48h; under 760.051 Torr; Inert atmosphere; Sealed tube;

With hydrogenchloride; water; In tetrahydrofuran; hexane; at 0 ℃; pH=< 2; regioselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1002/chem.201503359