{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

Base Information

Chemical Name:{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid
CAS No.:1333331-87-5
Molecular Formula:C₁₈H₁₇BN₂O₅
Molecular Weight:352.154
Hs Code.:

Synonyms:{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

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Chemical Property of {3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

Chemical Property:

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Technology Process of {3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

There total 12 articles about {3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333331-86-4
4'-iodo-3-[(4-methoxybenzyl)oxy]-4H-1,2'-bipyridin-4-one

: 1333331-87-5
{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

Guidance literature:: With potassium acetate; bis(pinacol)diborane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 100 ℃;

Reference yield:

: 1219-33-6
5-(benzyloxy)-4-oxo-4H-pyran-2-carboxylic acid

: 1333331-87-5
{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

Guidance literature:: Multi-step reaction with 6 steps

1: quinoline / 0.5 h / 235 °C / Reflux

2: hydrogenchloride / water / 2 h / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C

4: ammonia / water / 18 h / 100 °C / Sealed glass tube

5: potassium carbonate / dimethyl sulfoxide / 80 °C

6: bis(pinacol)diborane; potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C

With quinoline; hydrogenchloride; ammonia; potassium acetate; potassium carbonate; bis(pinacol)diborane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 61049-67-0
3-Benzyloxy-4-pyrone

: 1333331-87-5
{3-[(4-methoxybenzyl)oxy]-4-oxo-4H-1,2'-bipyridin-4-yl}boronic acid

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / water / 2 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 100 °C

3: ammonia / water / 18 h / 100 °C / Sealed glass tube

4: potassium carbonate / dimethyl sulfoxide / 80 °C

5: bis(pinacol)diborane; potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C

With hydrogenchloride; ammonia; potassium acetate; potassium carbonate; bis(pinacol)diborane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;