(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

Base Information

Chemical Name:(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N
CAS No.:706820-34-0
Molecular Formula:C₁₀₀H₁₅₀N₄
Molecular Weight:1408.32
Hs Code.:

(3,5-(2,4,6-(tert-butyl)3C<sub>6</sub>H<sub>2</sub>)2C<sub>6</sub>H<sub>3</sub>NHCH<sub>2</sub>CH<sub>2</sub>)2(4-(tert-butyl)C<sub>6</sub>H<sub>4</sub>NHCH<sub>2</sub>CH<sub>2</sub>)N

Synonyms:(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

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Chemical Property of (3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

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Technology Process of (3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

There total 1 articles about (3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 3972-65-4
1-bromo-4-tert-butylbenzene

: N-(2-amino-ethyl)-N'-(2,4,6,2'',4'',6''-hexa-tert-butyl-[1,1';3',1'']terphenyl-5'-yl)-N-[2-(2,4,6,2'',4'',6''-hexa-tert-butyl-[1,1';3',1'']terphenyl-5'-ylamino)-ethyl]-ethane-1,2-diamine

: 706820-34-0
(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

Guidance literature:: With tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene; at 110 ℃; for 48h;
DOI:10.1021/ja0306415

Reference yield: 39.0%

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 706820-34-0
(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NHCH₂CH₂)2(4-(tert-butyl)C₆H₄NHCH₂CH₂)N

: 709041-11-2
[(3,5-(2,4,6-(tert-butyl)3C₆H₂)2C₆H₃NCH₂CH₂)2(4-(tert-butyl)C₆H₄NCH₂CH₂)N]MoCl

Guidance literature:: With (Me₃Si)2NLi; In benzene; (N2); using Schlenk techniques; addn. of MoCl4(THF)2 to soln. of (3,5-(2,4,6-t-Bu3C6H2)2C6H3NHCH2CH2)2(4-t-BuC6H4NHCH2CH2)N in benzene for 20 min; stirring for 2 h at room temp.; addn. of (Me3Si)2NLi for 10 min; stirring for 4 h at room temp.; removal of solvent in vac., extn. with benzene, filtration, evapn. to dryness in vac., suspending in pentane, stirring vigorously for 20 min, concn., filtration, washing with cold pentane, elem. anal.;
DOI:10.1021/ja0306415