N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Base Information

Chemical Name:N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline
CAS No.:135685-07-3
Molecular Formula:C₂₅H₂₇N₃O₉
Molecular Weight:513.504
Hs Code.:

Synonyms:N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Suppliers and Price of N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

There total 4 articles about N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 135685-07-3
N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 4-(dimethylamino)pyridine (DMAP) / acetonitrile / 18 h / Ambient temperature

2: N-bromosuccinimide (NBS), dibenzoyl peroxide / CCl₄ / 20 h / Heating; Irradiation

3: Et₃N / acetonitrile / 6 h / Heating

With dmap; N-Bromosuccinimide; triethylamine; dibenzoyl peroxide; In tetrachloromethane; acetonitrile;
DOI:10.1021/jm00114a024

Reference yield:

: 135685-05-1
N,N-bis<(tert-butyloxy)carbonyl>-4-methyl-3-nitroaniline

: 135685-07-3
N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide (NBS), dibenzoyl peroxide / CCl₄ / 20 h / Heating; Irradiation

2: Et₃N / acetonitrile / 6 h / Heating

With N-Bromosuccinimide; triethylamine; dibenzoyl peroxide; In tetrachloromethane; acetonitrile;
DOI:10.1021/jm00114a024

Reference yield:

: 119-32-4
4-Methyl-3-nitroanilin

: 135685-07-3
N,N-bis<(tert-butyloxy)carbonyl>-3-nitro-4-<(phthalimidooxy)methyl>aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 4-(dimethylamino)pyridine (DMAP) / acetonitrile / 18 h / Ambient temperature

2: N-bromosuccinimide (NBS), dibenzoyl peroxide / CCl₄ / 20 h / Heating; Irradiation

3: Et₃N / acetonitrile / 6 h / Heating

With dmap; N-Bromosuccinimide; triethylamine; dibenzoyl peroxide; In tetrachloromethane; acetonitrile;
DOI:10.1021/jm00114a024