2,2-ditipylethenol

Base Information

• Chemical Name: 2,2-ditipylethenol
• CAS No.: 162897-17-8
• Molecular Formula: C₃₂H₄₈O
• Molecular Weight: 448.733

Synonyms:2,2-ditipylethenol

Chemical Property of 2,2-ditipylethenol

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-ditipylethenol

There total 9 articles about 2,2-ditipylethenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

ditipylketene (160778-07-4) → 2,2-ditipylethenol (162897-17-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/jo971049z

Reference yield: 67.0%

1,2-ditipylethanediol (198557-70-9) → 2,2-ditipylethenol (162897-17-8)

Guidance literature:

With hydrogenchloride; In acetic acid; for 3h; Heating;

DOI:10.1021/jo971049z

Reference yield:

→ 2,2-ditipylethenol (162897-17-8)

Guidance literature:

With ethanol; nickel; at 200 ℃; under 246395 Torr; unter Wasserstoff;

DOI:10.1021/ja01207a014

upstream raw materials:

1,2-ditipylethanediol

ditipylketene

2,2-bis(2,4,6-triisopropylphenyl)ethanal

sulfuric acid

Downstream raw materials:

2,2',4,4',6,6'-hexaisopropylbenzil

2,4,6,2',4',6'-Hexaisopropyl-benzoin

2,2-bis(2,4,6-triisopropylphenyl)ethanal

2,4,6,2',4',6'-hexaisopropyl-benzophenone

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