Technology Process of C17H28N3(1+)*F6P(1-)
There total 6 articles about C17H28N3(1+)*F6P(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H29N2O3S(1+)*F6P(1-);
With
sodium azide;
In
N,N-dimethyl-formamide;
at 80 ℃;
Inert atmosphere;
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
for 1h;
under 760.051 Torr;
Inert atmosphere;
DOI:10.1002/ejoc.201301366
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / Reflux
2.1: ammonium hexafluorophosphate / 0.25 h / 145 °C / Microwave irradiation; Inert atmosphere
3.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
4.1: sodium azide / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
4.2: 1 h / 760.05 Torr / Inert atmosphere
With
ammonium hexafluorophosphate; lithium aluminium tetrahydride; sodium azide; triethylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301366
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium hexafluorophosphate / 0.25 h / 145 °C / Microwave irradiation; Inert atmosphere
2.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.1: sodium azide / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
3.2: 1 h / 760.05 Torr / Inert atmosphere
With
ammonium hexafluorophosphate; sodium azide; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301366
