7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

Base Information

Chemical Name:7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole
CAS No.:1056265-26-9
Molecular Formula:C₂₁H₁₆ClFN₂O₂
Molecular Weight:382.822
Hs Code.:

Synonyms:7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

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Chemical Property of 7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

Chemical Property:

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Technology Process of 7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

There total 2 articles about 7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033810-99-9
7-chloro-4-(methyloxy)-1H-indazole

: 133057-83-7
4-benzyloxy-3-fluorophenylboronic acid

: 1056265-26-9
7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

: C₂₁H₁₆ClFN₂O₂

Guidance literature:: With pyridine; copper diacetate; In dichloromethane; for 96h; Molecular sieve;

Reference yield:

: 398456-81-0
3-chloro-2-fluoro-6-methoxybenzaldehyde

: 1056265-26-9
7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

: C₂₁H₁₆ClFN₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-methoxylamine hydrochloride; potassium carbonate / 1,2-dimethoxyethane / 4 h / 45 °C

1.2: Heating / reflux

2.1: pyridine / copper diacetate / dichloromethane / 96 h / Molecular sieve

With pyridine; N-methoxylamine hydrochloride; potassium carbonate; copper diacetate; In 1,2-dimethoxyethane; dichloromethane;

Reference yield:

: 1056265-26-9
7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole

: 1056262-61-3
7-chloro-1-(3-fluoro-4-hydroxyphenyl)-1H-indazol-4-ol

Guidance literature:: 7-chloro-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}-4-(methyloxy)-1H-indazole; With water; hydrogen bromide; for 2h; Heating / reflux;

With water; sodium hydrogencarbonate; pH=6;

With water; boron tribromide; sodium hydrogencarbonate; more than 3 stages;