4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

Base Information

Chemical Name:4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate
CAS No.:767332-38-7
Molecular Formula:C₁₈H₂₈O₃
Molecular Weight:292.419
Hs Code.:

Synonyms:4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

Suppliers and Price of 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

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Technology Process of 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

There total 2 articles about 4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 767332-37-6
4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-yn-1,4-diol

: 767332-38-7
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

Guidance literature:: With triethylamine; at 25 ℃; for 0.25h;
DOI:10.1002/hlca.200490155

Reference yield:

: 31499-72-6
7,8-dihydro-α-ionone

: 767332-38-7
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / KOH / tetrahydrofuran / 3.5 h / 15 °C

2: 92 percent / Et₃N / 0.25 h / 25 °C

With potassium hydroxide; triethylamine; In tetrahydrofuran;
DOI:10.1002/hlca.200490155

Reference yield:

: 767332-38-7
4-hydroxy-4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hex-2-ynyl cetate

: 767332-39-8
4-methyl-6-(2,6,6-trimethylcyclohex-2-en-1-yl)hexa-2,3-dien-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: TsOH*H₂O / toluene / 0.17 h / -20 °C

2: LiAlH₄ / toluene; tetrahydrofuran / 2 h / -50 - 20 °C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1002/hlca.200490155